1.
Laser radiation experiment
We will pass a laser beam through two different lattices, and compare the
"density" of the points obtained in the diffraction image. We will
measure the distances between the lattice lines with a microscope, on the basis
that each count in the microscope represents 0.01mm. We shall compare this
distance to the distance calculated from the diffraction image. We shall learn
on the reciprocal relation between the dimensions in the diffraction image and
the periodicity of the lattice.
2.
Single Crystal Experiment with X-ray radiation
General Description:
- The experimental system we will use is the rotating crystal method.
- The diffraction system on which the experiment is performed is the 4-circle
diffractometer, by Nonius, model
Mach3. The
experimental system is described in appendix
1. The ECON goniometer head, on which the
crystals will be
mounted is shown in appendix
2. The Eucentric goniometer head, onto which the capillary
powder
will be mounted, is shown in appendix 3.
The items described in the appendices are taken
from the Nonius7
company website.
In this experiment we will produce X-ray diffraction images of single crystals
of NaCl, KCl, and KBr, and also of NaCl powder.
The experiment includes the following steps: Learning to operate the diffraction system and the diffractometer
software, choosing the crystal and mounting it to the goniometer head, centering
the crystal and aligning it in
the path of the beam, installing the detector (polaroid
cassette), radiating the crystals with X-rays and
producing an image.
In the powder experiment, we will crush the
crystals into a powder, and
insert into a capillary attached to the goniometer head.
The capillary will be centered in the x-ray beam.
The results will be analyzed
according to the obtained diffraction images.
3.
Calculation of the cell dimensions and the plane indices by using the INDEX
software.
We will enter into the computer the x-y coordinates
of the diffraction
points, that are obtained on
the Polaroid diffraction image.
We shall operate the PHOTO procedure in order to center the values received in the image of the
rotation experiment. Eventually we will operate the
INDEX software that calculates the plane
indices and cell dimensions.
4.
Powder diffractometer experiment in the 2q/q
method
In this experiment we will radiate NaCl, KBr, and KCl powder with x-rays, and
obtain the typical
diffraction patterns ("finger prints") for each of
the materials, on a graph displaying the intensity as
a function of the diffraction angle, 2q.
The experimental system consists of a Miniflex
insrument, which is a compact
apparatus for x-ray
diffraction experiments, and a computer through which we determine the
conditions of the
experiment, and observe the diffraction patterns. The instrument contains a copper X-ray
tube, a
magnetic plate to hold the powder, filter (monochromator) and a radiation detector. The
voltage
and current settings of the tube are
constant and cannot be changed. Voltage-30kV, Current
15mA.